9,10; 9',10'; 9",10"-Hexahydro-[2.2.2](2,7)phenanthrenophan

Authors

  • W. Jenny Forschungslaboratorien der Ciba Aktiengesellschaft, Basel, Farbstoffabteilung; Institut für organische Chemie der Universität Bern
  • R. Paioni Forschungslaboratorien der Ciba Aktiengesellschaft, Basel, Farbstoffabteilung; Institut für organische Chemie der Universität Bern

DOI:

https://doi.org/10.2533/chimia.1968.248

Abstract

Starting from 2,7-diacetyl-9,10-dihydrophenanthrene, 2,7-dichloromethyl-9,10-dihydrophenanthrene was synthesized through a series of new compounds. The chromatographic separation of the crude product resulting from a modified Wurtz reaction with the dichloromethyl compound led to the isolation of 9,10; 9',10'; 9",10"-hexahydro-[2.2.2](2,7) phenanthrenophane, the structure of wich was confirmed by mass and NMR spectroscopy.

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Published

1968-05-31

Issue

Vol. 22 No. 5 (1968): Forschung/Research

Section

Kurze Mitteilungen

License

Copyright (c) 1968 W. Jenny

Creative Commons License

This work is licensed under a Creative Commons Attribution 4.0 International License.

How to Cite

[1]
W. Jenny, R. Paioni, Chimia 1968, 22, 248, DOI: 10.2533/chimia.1968.248.