Reaction Screening Using a Microreactor

FH – HES

Authors

  • Olivier Naef Ecole d'Ingénieurs et d'architectes de Fribourg Boulevard de Pérolles 80, CP 32, CH-1705 Fribourg
  • Mathieu Roch
  • Thierry Chappuis

DOI:

https://doi.org/10.2533/chimia.2010.889

Keywords:

Continuous mode, Esterification, Microreactor, Optimization, Screening

Abstract

This article discusses the screening of chemical reactions using a microreactor equipped with infrared spectroscopy as online analytics. An esterification reaction has been optimized in continuous mode with the proposed setup. The esterification did not work well due to the material of the microreactor (stainless-steel 316Ti) that catalyzed the decomposition of formic acid. However, despite the occurrence of decomposition, an optimization could be achieved with this system.
CHIMIA Vol. 64 No. 12 (2010): Vol. 64 No. 12 (2010): The 550th Anniversary of the University of Basel : Centuries of Excellence in Chemistry

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Published

2010-12-15

How to Cite

[1]
O. Naef, M. Roch, T. Chappuis, Chimia 2010, 64, 889, DOI: 10.2533/chimia.2010.889.

Issue

Vol. 64 No. 12 (2010): The 550th Anniversary of the University of Basel : Centuries of Excellence in Chemistry

Section

Columns, Conference Reports

Categories

License

Copyright (c) 2010 Swiss Chemical Society

Creative Commons License

This work is licensed under a Creative Commons Attribution-NonCommercial 4.0 International License.