Lösung eines stereochemischen Problems mit Hilfe moderner Methoden der hochauflösenden Kernresonanz

Authors

  • Peter Bigler

DOI:

https://doi.org/10.2533/chimia.1991.15

Abstract

Two powerful methods of high-resolution NMR spectroscopy have successfully been applied for the solution of a stereochemical problem. The advantages of a modified pulse sequence for heteronuclear 2D shift correlation with inverse mode of detection and of a new variant of homonuclear 1D-NOE spectroscopy, improved with respect to sensitivity and spectral quality, are demonstrated. These two methods allow structure elucidation by low sample amounts within reasonable measuring times.

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Published

1991-02-27